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Titel:

Quantitation of resveratrol in red wines by means of stable isotope dilution analysis-ultra-performance liquid chromatography-Quan-time-of-flight mass spectrometry and cross validation

Dokumenttyp:
Zeitschriftenaufsatz
Autor(en):
Stark, Timo; Wollmann, Nadine; Lösch, Sofie; Hofmann, Thomas
Abstract:
A stable isotope dilution analysis (SIDA) was developed for the quantitative analysis of the health-promoting phytoalexin (E)-resveratrol in red wines by means of UPLC-QuanTOF-MS. After hemisynthetic preparation of (E)-3,5,4'-trihydroxy-2,4,6-trideuterostilbene ((E)-[(2)H(3)]-resveratrol) as the stable isotope labeled internal standard, validation experiments revealed recovery rate of 96.2 +/- 0.8{%} RSD, thus demonstrating the robustness and accuracy of the SIDA-UPLC-QuanTOF-MS method. Repeatab...     »
Zeitschriftentitel:
Analytical Chemistry
Jahr:
2011
Band / Volume:
83
Heft / Issue:
9
Seitenangaben Beitrag:
3398--3405
Volltext / DOI:
doi:10.1021/ac103305s
Print-ISSN:
0003-2700
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