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Titel:

Simultaneous determination of cucurbitacin B, E, I and E-glucoside in plant material and body fluids by HPLC-MS.

Dokumenttyp:
Evaluation Studies; Journal Article
Autor(en):
Bajcsik, Nicole; Pfab, Rudolf; Pietsch, Jörg
Abstract:
A selective and sensitive analytical method for the simultaneous determination of cucurbitacin B, E, I and E-glucoside in plant material and body fluids by HPLC-MS was developed. After liquid-liquid extraction with dichlormethane, separation was achieved on a Phenomenex Luna Pentafluorophenyl Column (150mm×2mm, 5?m) using acetonitrile-water (90:10, v/v) as mobile phase system. Detection was performed using a 3200 Q Trap mass spectrometer (AB Sciex). For analysis Q1 Scans with negative ionisation...     »
Zeitschriftentitel:
J Chromatogr B Analyt Technol Biomed Life Sci
Jahr:
2017
Band / Volume:
1052
Seitenangaben Beitrag:
128-134
Sprache:
eng
Volltext / DOI:
doi:10.1016/j.jchromb.2017.03.030
PubMed:
http://view.ncbi.nlm.nih.gov/pubmed/28376351
Print-ISSN:
1570-0232
TUM Einrichtung:
2. Medizinische Klinik Toxikologische Abteilung (alt) (Prof. Zilker)
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