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Title:
Measurement of oxygen reduction activities via the rotating disc electrode method: From Pt model surfaces to carbon-supported high surface area catalysts
Abstract:
The aim of this report is to scrutinize the thin-film rotating disk electrode (TF-RDE) method for studying the electrocatalytic activity of high surface area catalysts. Special emphasis is given to the oxygen redn. reaction (ORR) on C-supported Pt catalysts. From measurements on 4 different Pt catalyst samples with various av. particle sizes, it is demonstrated in detail how the intrinsic properties of the catalyst, i.e., the mass activity (A/gPt) and the specific activity (A/m2Pt), are evaluate... »
Keywords:
Reduction catalysts (electrochem. polycryst. Pt to carbon-supported Pt nanoparticle for oxygen) Reduction (measurement of oxygen redn. activities via the rotating disk electrode method from polycryst. Pt to carbon-supported Pt nanoparticle high surface area catalysts) Nanoparticles Surface area (measurement of oxygen redn. activities via the rotating disk electrode method from polycryst. Pt to carbon-supported Pt nanoparticle high surface area catalysts in HClO4 soln.) Particle size (nanoscale m... »
Congress title:
CAN 148:412833 72-2 Electrochemistry Technische Universitaet Muenchen, Garching, Deutschland, Germany. Journal 0013-4686 7440-06-4 (Platinum); 7440-44-0 (Carbon) Role: CAT (Catalyst use), TEM (Technical or engineered material use), USES (Uses) (measurement of oxygen redn. activities via the rotating disk electrode method from polycryst. Pt to carbon-supported Pt nanoparticle high surface area catalysts); 7782-44-7 (Oxygen) Role: RCT (Reactant), RACT (Reactant or reagent) (measurement of oxygen... »
Journal title:
Electrochim. Acta
Year:
2008
Journal volume:
53
Journal issue:
7
Pages contribution:
3181-3188
Fulltext / DOI:
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